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3-methylcyclohex-2-en-1-yl acetate

  • Cas number：75411-49-3
  • purity：99%
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Product Details

3-methylcyclohex-2-en-1-yl acetate 75411-49-3 with purity >99% Low price in stock

  • Molecular Formula: C9H14 O2
  • Molecular Weight: 154.209
  • Vapor Pressure: 0.486mmHg at 25°C 
  • Boiling Point: 192.5°C at 760 mmHg 
  • Flash Point: 60.5°C 
  • PSA： 26.30000 
  • Density: 0.98g/cm3 
  • LogP: 2.04830 

3-methylcyclohex-2-en-1-yl acetate(Cas 75411-49-3) Usage

Synthesis Reference(s)

Tetrahedron Letters, 25, p. 4187, 1984 DOI: 10.1016/S0040-4039(01)81391-5

InChI:InChI=1/C9H14O2/c1-7-4-3-5-9(6-7)11-8(2)10/h6,9H,3-5H2,1-2H3

75411-49-3 Relevant articles

Ein einfacher und allgemeiner Zugang zu 2-Fluor-1,3-dienen

Spahic, Bojana,Thu, Truong Thi My,Schlosser, Manfred

, p. 1236 - 1241 (1980)

Upon treatment of 1- chloro-1-fluoro-2-h...

Metal-free, aerobic dioxygenation of alkenes using hydroxamic acids

Schmidt, Valerie A.,Alexanian, Erik J.

supporting information; scheme or table, p. 4491 - 4494 (2010/08/21)

(Chemical equation presented) One dioxyg...

Oxidative esterification of alkenes via π- and σ-organopalladium complexes: New pathways for the reaction

Kozitsyna, N.Yu.,Bukharkina,Martens,Vargaftik,Moiseev

, p. 69 - 75 (2007/10/03)

New mechanistic data on the oxidative es...

KF-Al2O3 is an efficient solid support reagent for the acetylation of amines, alcohols, and phenols. Impeding effect of solvent on the reaction rate

Yadav, Veejendra K,Ganesh Babu,Mittal, Manish

, p. 7047 - 7051 (2007/10/03)

KF-Al2O3 brings about rapid acetylation ...

Pd-containing catalytic system for oxidative acetoxylation of alkenes

Romanenko,Tormyshev,Shteingarts

, p. 1549 - 1562 (2007/10/03)

Four-substituted cyclohexenes were used ...

75411-49-3 Process route

1-methylcyclohex-1-ene
591-49-1

1-methylcyclohex-1-ene

acetic acid
64-19-7,77671-22-8

acetic acid

2-methyl-2-cyclohexen-1-yl acetate
13295-90-4

2-methyl-2-cyclohexen-1-yl acetate

3-methyl-2-cyclohexen-1-yl acetate
75411-49-3

3-methyl-2-cyclohexen-1-yl acetate

Conditions
Conditions Yield
With 2-Methoxyacetophenone; p-benzoquinone; palladium(II) trifluoroacetate; at 60 ℃; for 1h; Yield given. Yields of byproduct given;
With copper diacetate; oxygen; hydroquinone; palladium diacetate; at 50 ℃; under 760 Torr;
37 % Turnov.
63 % Turnov.
With tetraethylammonium tosylate; (electrolysis);
With cobalt(III) acetate; at 39.9 ℃; for 24h;
1 % Chromat.
59 % Chromat.
With p-benzoquinone; palladium diacetate; at 50 - 60 ℃; for 24h; Title compound not separated from byproducts;
3-methylcyclohex-2-en-1-ol
21378-21-2,54423-21-1

3-methylcyclohex-2-en-1-ol

acetic anhydride
108-24-7

acetic anhydride

3-methyl-2-cyclohexen-1-yl acetate
75411-49-3

3-methyl-2-cyclohexen-1-yl acetate

Conditions
Conditions Yield
With pyridine; at 25 ℃; for 12h;
88%
With pyridine; for 96h; Ambient temperature;
With pyridine;
With pyridine; dmap; In dichloromethane;

75411-49-3 Upstream products

  • 591-49-1
    591-49-1

    1-methylcyclohex-1-ene

  • 64-19-7
    64-19-7

    acetic acid

  • 591-48-0
    591-48-0

    3-methyl-1-cyclohexene

  • 90498-69-4
    90498-69-4

    Acetat des 1-Methyl-cyclohexen-(2) -ols-(1)

75411-49-3 Downstream products

  • 21378-21-2
    21378-21-2

    3-methylcyclohex-2-en-1-ol

  • 22597-21-3
    22597-21-3

    M-Cresyl acetate

  • 18890-22-7
    18890-22-7

    (R)-3-methylcyclohex-2-en-1-ol

  • 60733-10-0
    60733-10-0

    (S)-seudenol

3-methylcyclohex-2-en-1-yl acetate

CAS:75411-49-3

Purity:99%

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